File:Small-scale determination of ammoniacal nitrogen in fertilizers (Alessandri 1895.31).png
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DescriptionSmall-scale determination of ammoniacal nitrogen in fertilizers (Alessandri 1895.31).png |
Italiano: Una campana C con foro superiore è posta su di una superficie con scanalatura a chiusura ermetica a mercurio. Al suo interno vi è un cristallizzatore D con una quantità nota di soluzione di un acido non volatile. Sopra un treppiede vi è una capsula E con una piccola quantità di concime o sale ammoniacale. La campana viene posta sotto vuoto tramite un rubinetto F. Quando la campana è sotto vuoto, si fa gocciolare nella capsula una soluzione di idrossido di potassio KOH da una pipetta H, G. Si lascia il tutto a riposare per 24 h affinché la decomposizione abbia luogo e l'ammoniaca liberata venga assorbita dalla soluzione acida. Infine, la soluzione viene titolata per ricavare l'ammoniaca assorbita.
English: A glass bell C with a top aperture is placed on a surface with a groove that allows an ermetic seal, possibly under mercury. Inside is a dish D with a known amount of a non-volatile acid solution, and above it a capsule E with a small amount of an ammoniacal salt or a fertiliser. The bell is evacuated via F, and a solution of potassium hydroxide KOH is added dropwise to the capsule via a pipette G, H. The system is allowed to react for 24 h until all the ammonia is released by the sample and absorbed by the acid solution, which is then titrated. |
Date | |
Source | Alessandri, P. E. Analisi Volumetrica Applicata Ai Prodotti Commerciali e Industriali; Ulrico Hoepli: Milano, 1895. |
Author | valeg96 |
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Public domainPublic domainfalsefalse |
This work is in the public domain in its country of origin and other countries and areas where the copyright term is the author's life plus 70 years or fewer. This work is in the public domain in the United States because it was published (or registered with the U.S. Copyright Office) before January 1, 1929. | |
This file has been identified as being free of known restrictions under copyright law, including all related and neighboring rights. |
https://creativecommons.org/publicdomain/mark/1.0/PDMCreative Commons Public Domain Mark 1.0falsefalse
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File change date and time | 19:43, 24 August 2020 |
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