File:Synthesis of Tetrachlorobis(diethyl ether)molybdenum(IV) - MoCl4(OEt2)2.webm

Synthesis_of_Tetrachlorobis(diethyl_ether)molybdenum(IV)_-_MoCl4(OEt2)2.webm(WebM audio/video file, VP8/Vorbis, length 11 min 1 s, 640 × 360 pixels, 874 kbps overall, file size: 68.81 MB)

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Description Synthesis of MoCl4(OEt2)2. In this episode, the conversion is illustrated of commercially available MoCl5 to MoCl4(OEt2)2 using tin shot as the reducing agent. The preparation is carried out by Dr. John J. Curley in the Cummins laboratory at MIT. The procedure is a modification of one reported originally by Poli et al.: Eur. J. Inorg. Chem. 2001, 2699-2703 doi:10.1002/1099-0682(200109)2001:10<2699::AID-EJIC2699>3.0.CO;2-S
Date
Source Molybdenum tetrachloride bis(diethyl ether)
Author ccclabmit
Media of the day This file was selected as the media of the day for 23 March 2014. It was captioned as follows:
English: Synthesis of MoCl4(OEt2)2. In this episode, the conversion is illustrated of commercially available MoCl5 to MoCl4(OEt2)2 using tin shot as the reducing agent.
Other languages
English: Synthesis of MoCl4(OEt2)2. In this episode, the conversion is illustrated of commercially available MoCl5 to MoCl4(OEt2)2 using tin shot as the reducing agent.
中文(简体):用锡还原五氯化钼合成四氯化钼乙醚络合物

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This file, which was originally posted to Molybdenum tetrachloride bis(diethyl ether), was reviewed on 20 March 2014 by reviewer Indeedous, who confirmed that it was available there under the stated license on that date.
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This file is licensed under the Creative Commons Attribution 3.0 Unported license.
Attribution: ccclabmit
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Date/TimeThumbnailDimensionsUserComment
current17:32, 20 March 201411 min 1 s, 640 × 360 (68.81 MB)Jacopo Werther (talk | contribs)== {{int:filedesc}} == {{Information |Description = Synthesis of MoCl4(OEt2)2. In this episode, the conversion is illustrated of commercially available MoCl5 to MoCl4(OEt2)2 using tin shot as the reducing agent. The preparation is carried out by Dr....

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Format Bitrate Download Status Encode time
VP9 360P 534 kbps Completed 04:31, 21 October 2018 11 min 28 s
Streaming 360p (VP9) Not ready Unknown status
VP9 240P 319 kbps Completed 04:29, 21 October 2018 9 min 45 s
Streaming 240p (VP9) 228 kbps Completed 05:40, 17 December 2023 3.0 s
WebM 360P 564 kbps Completed 17:47, 20 March 2014 14 min 47 s
Streaming 144p (MJPEG) 1 Mbps Completed 01:23, 20 November 2023 16 s
Stereo (Opus) 87 kbps Completed 03:31, 24 November 2023 9.0 s
Stereo (MP3) 128 kbps Completed 01:24, 20 November 2023 17 s